Resumo Introdução A evolução dos sistemas adesivos permitiu que os fabricantes desenvolvessem materiais com técnicas cada vez mais simplificadas, porém que, ainda assim, promovessem adequados valores de resistência de união imediata. Sugere-se que alguns tratamentos da superfície dentinária podem favorecer esse processo de adesão. Objetivo Avaliar os efeitos de diferentes tratamentos, em superfície dentinária plana condicionada, sobre a resistência de união à microtração de sistemas adesivos do tipo “condiciona-e-lava” de dois passos. Material e método Noventa e seis terceiros molares humanos foram divididos em 12 grupos (n=8), aleatoriamente, de acordo com o sistema adesivo utilizado (GI: Adper Single Bond 2 - 3M ESPE; GII: Prime & Bond 2.1 - Dentsply; GIII: Excite - Ivoclar Vivadent) e o tipo de tratamento do substrato dentinário condicionado (a: água; b: clorexidina + água; c: etanol; d: clorexidina + etanol). Todos os dentes foram restaurados com resina Charisma na cor A2 (Heraeus - Kulzer, Germany) e submetidos a ensaio mecânico de microtração (EMIC DL-2000). O teste estatístico realizado foi ANOVA a um fator, completado com teste de Tukey. Resultado Os grupos GIIc, GIIIc e GIId apresentaram aumento significativo estatisticamente na resistência de união à microtração imediata. Conclusão Os diferentes tratamentos da dentina condicionada não afetaram de maneira negativa a resistência de união para todos os sistemas adesivos testados e a utilização da técnica com etanol, associado ou não à clorexidina, parece ser uma interessante abordagem quando associada a sistemas adesivos “condiciona-e-lava” de dois passos.

Abstract Introduction The development of adhesive systems allow manufacturers to develop materials with increasingly simplified techniques, but that still would promote adequate resistance values of immediate union. It is suggested that some treatments of dentin surface can facilitate the process of accession. Objective To evaluate the effects of different treatments in conditioned flat dentin surface on bond strength to microtensile 2-step etch-and-rinse adhesive systems. Material and method Ninety-six human third molars were divided into twelve groups (n = 8) randomly according to the used adhesive system (GI: Single Bond 2 - 3M ESPE; GII: Prime & Bond 2.1 - Dentsply; GIII: Excite - Ivoclar Vivadent) and type of treatment of the conditioned dentin (a: water; b: water + chlorhexidine; c: ethanol; d: chlorhexidine + ethanol). All teeth were restored with Charisma color A2 (Heraeus – Kulzer, Germany) and subjected to mechanical testing microtensile (EMIC DL-2000). The statistical test performed was ANOVA 1 factor supplemented with Tukey test. Result GIIc groups GIIIc and GIId showed statistically significant increase in bond strength to immediate microtensile. Conclusion The different treatments of dentin did not affect negatively the bond strength for all tested adhesive systems and the use of the technique with ethanol, with or without chlorhexidine, appears to be an interesting approach when combined with 2-step etch-and-rinse adhesive systems.

Abstract This study evaluated the effects of 10% alphatocopherol on the fracture resistance of endodontically treated teeth subjected to tooth bleaching with hydrogen peroxide and immediately restored with composite resin. Fifty bovine incisors were selected, including 10 sound teeth that constituted the control group (G1 (C)). The remaining 40 teeth, which were endodontically treated, were divided into four groups (n = 10): G2 (CR), consisting of teeth immediately restored with composite resin; G3 (HP + CR), consisting of teeth subjected to tooth bleaching with 38% hydrogen peroxide and immediately restored with composite resin; G4 (HP + SA + CR), which received treatment similar to that used for G3, but with 10% sodium ascorbate gel applied after the bleaching protocol; and G5 (HP + AT + CR), which was similar to G4 but included 10% alphatocopherol gel as an antioxidant. After 24 h, composite restorations were performed, and teeth were subjected to a fracture resistance test at a speed of 0.5 mm/min in an electromechanical testing machine. The axial force was applied with an angle of incidence of 135° relative to the long axis of the root. Data were subjected to ANOVA and Tukey tests (p = 0.05). G1 exhibited the highest fracture resistance (p < 0.05). No significant differences among the other experimental groups were observed. The 10% sodium ascorbate and 10% alphatocopherol gels did not improve the fracture resistance of endodontically treated teeth subjected to bleaching with 38% hydrogen peroxide.

O objetivo deste estudo foi o de avaliar in vitro a resistência adesiva de bráquetes após o pré-tratamento do esmalte com diferentes soluções fluoretadas. Foram utilizados 48 incisivos bovinos hígidos recém-extraídos que foram aleatoriamente divididos em 4 grupos experimentais (n=12). CG (controle): sem tratamento; FN: aplicação de flúor neutro por 4 min; FFA: aplicação de flúor fosfato acidulado (FFA) a 1,23% por 4 min; e VFS: aplicação de verniz de fluoreto de sódio a 5% por 6 h. Após o tratamento dos grupos, foi realizada a profilaxia do esmalte e os bráquetes foram fixados utilizando o compósito Transbond XT (3M), seguindo as especificações do fabricante. A resistência adesiva foi verificada através do teste de cisalhamento, realizado na Máquina de Ensaio Universal DL-2000 24 h após a fixação dos bráquetes. As superfícies dos dentes foram analisadas para verificação do índice de adesivo remanescente (IAR). Por meio dos testes estatísticos ANOVA e Tukey (α=5%), observou-se diferença estatisticamente significante entre os grupos estudados (p<0,0001), sendo que GC e FN, apresentaram valores superiores de resistência adesiva quando comparados aos grupos FFA e VFS, porém GC-NF e FFA-VFS não apresentaram diferenças estatisticas entre si (p>0,05). A análise dos escores do IAR revelou que grande parte das falhas ocorreram na interface esmalte-resina. Conclui-se que o tratamento do esmalte com FFA 1,23% e VFS a 5%, previamente à fixação de bráquetes ortodônticos, reduziu os valores de resistência adesiva ao cisalhamento

The aim of this in vitro study was to evaluate the shear bond strength of brackets after pre-treatment with different fluoride solutions. This study used 48 freshly extracted sound bovine incisors that were randomly assigned to 4 experimental groups (n=12). CG: (control) without treatment; NF: 4 min application of neutral fluoride; APF: application of 1.23% acidulated phosphate fluoride (APF) for 4 min; and SFV: application of 5% sodium fluoride varnish for 6 h. For each group, after surface treatment, prophylaxis of enamel and bracket bonding with Transbond XT composite resin (3M) were performed following the manufacturer's specifications. The shear bond strength was performed with a universal testing machine 24 h after fixing the brackets. The tooth surfaces were analyzed to verify the adhesive remnant index (ARI). Data were analyzed statistically by ANOVA and Tukey's test (α=0.05). There was statistically significant difference among the groups (p<0.0001). CG and NF groups presented significantly higher bond strength than APF and SFV. There was no significant difference between CG and NF or between APF and SFV (p>0.05). The analysis of ARI scores revealed that most failures occurred at the enamel-resin interface. It may be concluded that the pre-treatment of enamel with 1.23% APF and 5% SFV prior to fixing orthodontic brackets reduces shear bond strength values.